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Pulsed laser deposition (PLD) is widely used
in the materials processing industry. With this technique, multi-component
materials can be ablated from the the target and deposited onto a substrate to form
stoichiometric layers which match the target material. A basic
PLD system has been set up at Colorado State University. Figures
show a schematic diagram of the CSU system. A krypton fluoride
(KrF) excimer laser with a wavelength of 248 nm (Lambda Physik
model LPX 305 i) is used as the energy source. The maximum output energy
of the laser is about 1200 mJ per pulse at a pulse duration
of 25 ns. The maximum repetition rate is 50 Hz. The laser beam
is focused into a rotating target stage and it is rastered using a
stepper motor driven mirror. The target angle of incidence
is 45 degrees. The laser spot size on the target surface is
about 0.1 mm2. A mechanical rotary pump (HyVac 55L)
and a turbomolecular pump (Electrorava ) are used to evacuate
the vacuum chamber. The chamber can be pumped down to a base
pressure of 2.5 X 10-7 Torr. A baratron (MKS 127A)
and ionization gauge are used to detect the pressure of
the chamber in a range 10-3 - 10-7 Torr.
The oxygen pressure in chamber is controlled with an MKS 651C
pressure controller and an MKS 247C four-channel readout. The
substrate heater (Blue Wave Semiconductor) can be operated from
high vacuum (10-7 Torr) up to an oxygen pressure
of 1 atmosphere. The maximum temperature of operation in vacuum
or in an oxygen atmosphere is 900 oC. The substrate
heater can be used at temperatures up to 950 oC for
short periods (up to 30 min).
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